1 |
The exchange equilibrium in gas chromatography depends on. |
Solubility or absorbability of he sample
The polarity of he stationary phase and analyte
The degree of H bonding
All above factors
|
2 |
Which of the following techniques is used to separate a mixture of cations. |
GC
FPLC
Ion exchange chromatography
Size exchange chromatography
|
3 |
Which of the following techniques is used for the separation of macromolecules polymers. |
Size exclusion chromatogrphy
TLC
GLC
HPLC
|
4 |
Which of the following technique is used for separation of volatile components. |
GC
HPLC
FPLC
TLC
|
5 |
Which of the following factor is involved in band boarding that occur in column chromatography. |
Number of theoretical plates
Eddy diffusion
In phase mass transfer
All above
|
6 |
The plate height is the length of the column divide by |
Length of the column
Width of the column
Number of theoretical plates
Number of components of the mixture.
|
7 |
The theoretical plate in chromatography is represented by how many equilibrium step |
One
Two
Three
Four
|
8 |
The separation efficiency of a column can be expressed in terms of number of. |
Solvents used
Theoretical plates
Stationary phases
Mobile phases
|
9 |
Which of the following techniques involve gas as the mobile phase. |
HPLC
GLC
TLC
Paper chromatography
|
10 |
In which of the following techniques the solvated molecules are separated according to their size by their ability to penetrate a sieve like structure. |
Adsorption chromatography
Partition chromatography
Ion exchange chromatography
Gel permeation chromatography
|
11 |
Which of the following techniques involves ion exchange phenomenon. |
Size exclusion chromatography
Ion exchange chromatography
GLC
HPLC
|
12 |
In reverse phase chromatography which of the analyte will be eluted more readily. |
Polar
Non polar
Semi polar
All above
|
13 |
In reverse phase chromatography which of the analyte will be retained more on the stationary phase. |
Semi polar
Non polar
Polar
None of the above
|
14 |
In normal mode of operations of liquid liquid partition, a polar stationary phase is used with a non polar mobile phase Which of the following solvent is used as mobile phase. |
Ethanol
Propanol
Butanol
Hexane
|
15 |
TLC belongs to which of the following chromatographic techniques. |
Ion exchange
Partities chromatography
Adsorption chromatography
Gel permeation
|
16 |
Which of the following basic process is involved in the separation of the complex mixture by chromatographic techique. |
Partition
Adsorptions
Ion exchange
All of the above processes
|
17 |
Which of the following techniques does not belong to column chromatographyy |
TLC
HPLC
Electrophoresis
Ion exchange
|
18 |
The chemical method of separation in which the analytes to be separated are distributed between two phases, one of which is stationary phase while the other moves in a definite direction This technique is known as. |
Electrophoreals
Chromatography
Solvent extraction
Catachreals
|
19 |
Solid phase micro extraction is a solvent less extraction technique This technique is used for preparation of samples for analysis by which of the following technique. |
HPLC
GC
TLC
Electrophoreals
|
20 |
Beside the common silica based SPE particles, polymer supports are also available They have advantages over silica based SPE particles, Which of the following reason is possible. |
These are stable over a wide pH range.
These do not possesses residual silica groups
These are designed to be wettable and have high capacity than silica base particles.
All above
|
21 |
Which of the following extractant is used to solid phase extraction |
Bonding of C18 chains on silica
Bonding of C20 on paper
Bonding of C18 on glass
Bonding of C20 on cellulose
|
22 |
Which of the following interaction is involved in solid phase extraction technique. |
Van der Waals forces
Dipolar attraction
H bonding
All of above
|
23 |
The most widely used method of extracting metal ions is the formation of a chelate molecule with an organic chelating agent The chelating agents are. |
Strong acids
Strong bases
Weak bases
Weak acids
|
24 |
Which of the following technique is useful to remove metal ions from an interfering matrix. |
Solvent extraction
Electrophorests
Cataphorests
Gel permeation
|
25 |
When a solute is dissolved in two immiscible solvents it will distributes itself between two phases and the ratio of the concentration of the solute in two phases will be constant, This is known as. |
Starke law
Distribution law
Equilibrium law
Snell's law
|
26 |
Which of the following techniques is used to reduce the need for large volumes of organic solvents. |
Solid phase extraction
Gel permeation
Electrophoresis
TLC
|
27 |
Which of the following technique involves the bonding of hydrophobic functional group to solid particle, surface and acts as extracting phase |
Liquid phase extraction
Solid phase extraction
Electrophoresis
Gel electrophoresis
|
28 |
Which of the following techniques involves the distribution of solute between two immiscible liquid phases. |
Chromatography
Electrophoresis
Solvent extractions
Solid phase extraction
|
29 |
Which of the following techniques is used for cleanup of samples prior to introduction into chromatographic column. |
Paper chromatography
TLC
Solvnent extraction
Solid phase extraction
Both C and D
|
30 |
Which of the following source is commonly used as excitation source in fluorimeter. |
Tungsten lamp
Mercury vapour lamp
Nernst vapur lamp
Radio souse
|